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Published in: Head & Face Medicine 1/2017

Open Access 01-12-2017 | Research

Effect of aging and curing mode on the compressive and indirect tensile strength of resin composite cements

Authors: Nadja Rohr, Jens Fischer

Published in: Head & Face Medicine | Issue 1/2017

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Abstract

Background

Resin composite cements are used in dentistry to bond ceramic restorations to the tooth structure. In the oral cavity these cements are subjected to aging induced by masticatory and thermal stresses. Thermal cycling between 5 and 55 °C simulates the effect of varying temperatures in vitro. Purpose of this study was to compare indirect tensile to compressive strength of different cements before and after thermal cycling. The effect of the curing mode was additionally assessed.

Methods

Indirect tensile strength and compressive strength of 7 dual-curing resin composite cements (Multilink Automix, Multilink SpeedCem, RelyX Ultimate, RelyX Unicem 2 Automix, Panavia V5, Panavia SA Plus, Harvard Implant semi-permanent) was measured. The specimens were either autopolymerized or light-cured (n = 10). The mechanical properties were assessed after 24 h water storage at 37 °C and after aging (20,000 thermo cycles) with previous 24 h water storage at 37 °C.

Results

Indirect tensile strength ranged from 5.2 ± 0.8 to 55.3 ± 4.2 MPa, compressive strength from 35.8 ± 1.8 MPa to 343.8 ± 19.6 MPa.

Conclusions

Thermocyclic aging of 20,000 cycles can be considered a suitable method to simulate the degradation of indirect tensile strength but not compressive strength of resin composite cements. The effect of thermocycling and the curing mode on the resin composite cements is material dependent and cannot be generalized.
Literature
1.
go back to reference Ban S, Hasegawa J, Anusavice KJ. Effect of loading conditions on bi-axial flexure strength of dental cements. Dent Mater. 1992;8:100–4.CrossRefPubMed Ban S, Hasegawa J, Anusavice KJ. Effect of loading conditions on bi-axial flexure strength of dental cements. Dent Mater. 1992;8:100–4.CrossRefPubMed
2.
go back to reference Peutzfeldt A. Dual-cure resin cements: in vitro wear and effect of quantity of remaining double bonds, filler volume, and light curing. Acta Odontol Scand. 1995;53:29–34.CrossRefPubMed Peutzfeldt A. Dual-cure resin cements: in vitro wear and effect of quantity of remaining double bonds, filler volume, and light curing. Acta Odontol Scand. 1995;53:29–34.CrossRefPubMed
3.
go back to reference Ilie N, Simon A. Effect of curing mode on the micro-mechanical properties of dual-cured self-adhesive resin cements. Clin Oral Investig. 2012;16:505–12.CrossRefPubMed Ilie N, Simon A. Effect of curing mode on the micro-mechanical properties of dual-cured self-adhesive resin cements. Clin Oral Investig. 2012;16:505–12.CrossRefPubMed
4.
go back to reference Attar N, Tam LE, McComb D. Mechanical and physical properties of contemporary dental luting agents. J Prosthet Dent. 2003;89:127–34.CrossRefPubMed Attar N, Tam LE, McComb D. Mechanical and physical properties of contemporary dental luting agents. J Prosthet Dent. 2003;89:127–34.CrossRefPubMed
5.
go back to reference Diaz-Arnold AM, Vargas MA, Haselton DR. Current status of luting agents for fixed prosthodontics. J Prosthet Dent. 1999;81:135–41.CrossRefPubMed Diaz-Arnold AM, Vargas MA, Haselton DR. Current status of luting agents for fixed prosthodontics. J Prosthet Dent. 1999;81:135–41.CrossRefPubMed
6.
go back to reference Zandinejad AA, Atai M, Pahlevan A. The effect of ceramic and porous fillers on the mechanical properties of experimental dental composites. Dent Mater. 2006;22:382–7.CrossRefPubMed Zandinejad AA, Atai M, Pahlevan A. The effect of ceramic and porous fillers on the mechanical properties of experimental dental composites. Dent Mater. 2006;22:382–7.CrossRefPubMed
7.
go back to reference White SN, Yu Z. Physical properties of fixed prosthodontic, resin composite luting agents. Int J Prosthodont. 1993;6:384–9.PubMed White SN, Yu Z. Physical properties of fixed prosthodontic, resin composite luting agents. Int J Prosthodont. 1993;6:384–9.PubMed
8.
go back to reference Asmussen E, Peutzfeldt A. Influence of UEDMA BisGMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater. 1998;14:51–6.CrossRefPubMed Asmussen E, Peutzfeldt A. Influence of UEDMA BisGMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater. 1998;14:51–6.CrossRefPubMed
9.
go back to reference Müller JA, Rohr N, Fischer J. Evaluation of ISO 4049: water sorption and water solubility of resin cements. Eur J Oral Sci. 2017;125:141–50.CrossRefPubMed Müller JA, Rohr N, Fischer J. Evaluation of ISO 4049: water sorption and water solubility of resin cements. Eur J Oral Sci. 2017;125:141–50.CrossRefPubMed
10.
go back to reference Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci. 1997;105:97–116.CrossRefPubMed Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci. 1997;105:97–116.CrossRefPubMed
11.
go back to reference De Munck J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto-adhesive luting material to enamel and dentin. Dent Mater. 2004;20:963–71.CrossRefPubMed De Munck J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto-adhesive luting material to enamel and dentin. Dent Mater. 2004;20:963–71.CrossRefPubMed
12.
go back to reference Monticelli F, Osorio R, Mazzitelli C, Ferrari M, Toledano M. Limited decalcification/diffusion of self-adhesive cements into dentin. J Dent Res. 2008;87:974–9.CrossRefPubMed Monticelli F, Osorio R, Mazzitelli C, Ferrari M, Toledano M. Limited decalcification/diffusion of self-adhesive cements into dentin. J Dent Res. 2008;87:974–9.CrossRefPubMed
13.
go back to reference Rohr N, Fischer J. An evaluation of tooth surface treatment strategies for adhesive cementation - an elaborated primer supersedes tooth etching. J Adv Prosthodont. 2017;9:85–92.CrossRefPubMedPubMedCentral Rohr N, Fischer J. An evaluation of tooth surface treatment strategies for adhesive cementation - an elaborated primer supersedes tooth etching. J Adv Prosthodont. 2017;9:85–92.CrossRefPubMedPubMedCentral
14.
go back to reference Piwowarczyk A, Lauer HC. Mechanical properties of luting cements after water storage. Oper Dent. 2003;28:535–42.PubMed Piwowarczyk A, Lauer HC. Mechanical properties of luting cements after water storage. Oper Dent. 2003;28:535–42.PubMed
15.
go back to reference Caughman WF, Chan DC, Rueggeberg FA. Curing potential of dual-polymerizable resin cements in simulated clinical situations. J Prosthet Dent. 2001;85:479–84.CrossRefPubMed Caughman WF, Chan DC, Rueggeberg FA. Curing potential of dual-polymerizable resin cements in simulated clinical situations. J Prosthet Dent. 2001;85:479–84.CrossRefPubMed
16.
go back to reference Braga RR, Condon JR, Ferracane JL. Vitro wear simulation measurements of composite versus resin-modified glass ionomer luting cements for all-ceramic restorations. J Esthet Restor Dent. 2002;14:368–76.CrossRefPubMed Braga RR, Condon JR, Ferracane JL. Vitro wear simulation measurements of composite versus resin-modified glass ionomer luting cements for all-ceramic restorations. J Esthet Restor Dent. 2002;14:368–76.CrossRefPubMed
17.
go back to reference Fonseca RG, Santos JG, Adabo GL. Influence of activation modes on diametral tensile strength of dual-curing resin cements. Braz Oral Res. 2005;19:267–71.CrossRefPubMed Fonseca RG, Santos JG, Adabo GL. Influence of activation modes on diametral tensile strength of dual-curing resin cements. Braz Oral Res. 2005;19:267–71.CrossRefPubMed
18.
go back to reference Cantoro A, Goracci C, Papacchini F, Mazzitelli C, Fadda GM, Ferrari M. Effect of pre-cure temperature on the bonding potential of self-etch and self-adhesive resin cements. Dent Mater. 2008;24:577–83.CrossRefPubMed Cantoro A, Goracci C, Papacchini F, Mazzitelli C, Fadda GM, Ferrari M. Effect of pre-cure temperature on the bonding potential of self-etch and self-adhesive resin cements. Dent Mater. 2008;24:577–83.CrossRefPubMed
19.
go back to reference Cantoro A, Goracci C, Carvalho CA, Coniglio I, Ferrari M. Bonding potential of self-adhesive luting agents used at different temperatures to lute composite onlays. J Dent. 2009;37:454–61.CrossRefPubMed Cantoro A, Goracci C, Carvalho CA, Coniglio I, Ferrari M. Bonding potential of self-adhesive luting agents used at different temperatures to lute composite onlays. J Dent. 2009;37:454–61.CrossRefPubMed
20.
go back to reference Spinell T, Schedle A, Watts DC. Polymerization shrinkage kinetics of dimethacrylate resin-cements. Dent Mater. 2009;25:1058–66.CrossRefPubMed Spinell T, Schedle A, Watts DC. Polymerization shrinkage kinetics of dimethacrylate resin-cements. Dent Mater. 2009;25:1058–66.CrossRefPubMed
21.
go back to reference De Souza G, Braga RR, Cesar PF, Lopes GC. Correlation between clinical performance and degree of conversion of resin cements: a literature review. J Appl Oral Sci. 2015;23:358–68.CrossRefPubMedPubMedCentral De Souza G, Braga RR, Cesar PF, Lopes GC. Correlation between clinical performance and degree of conversion of resin cements: a literature review. J Appl Oral Sci. 2015;23:358–68.CrossRefPubMedPubMedCentral
22.
go back to reference Blumer L, Schmidli F, Weiger R, Fischer JA. Systematic approach to standardize artificial aging of resin composite cements. Dent Mater. 2015;31:855–63.CrossRefPubMed Blumer L, Schmidli F, Weiger R, Fischer JA. Systematic approach to standardize artificial aging of resin composite cements. Dent Mater. 2015;31:855–63.CrossRefPubMed
23.
go back to reference Fonseca RG, Artusi TP, dos Santos JG, Adabo GL. Diametral tensile strength of dual-curing resin cements submitted exclusively to autopolymerization. Quintessence Int. 2007;38:e527–31.PubMed Fonseca RG, Artusi TP, dos Santos JG, Adabo GL. Diametral tensile strength of dual-curing resin cements submitted exclusively to autopolymerization. Quintessence Int. 2007;38:e527–31.PubMed
24.
go back to reference White SN, Yu Z. Compressive and diametral tensile strengths of current adhesive luting agents. J Prosthet Dent. 1993;69:568–72.CrossRefPubMed White SN, Yu Z. Compressive and diametral tensile strengths of current adhesive luting agents. J Prosthet Dent. 1993;69:568–72.CrossRefPubMed
25.
go back to reference Stawarczyk B, Beuer F, Ender A, Roos M, Edelhoff D, Wimmer T. Influence of cementation and cement type on the fracture load testing methodology of anterior crowns made of different materials. Dent Mater J. 2013;32:888–95.CrossRefPubMed Stawarczyk B, Beuer F, Ender A, Roos M, Edelhoff D, Wimmer T. Influence of cementation and cement type on the fracture load testing methodology of anterior crowns made of different materials. Dent Mater J. 2013;32:888–95.CrossRefPubMed
26.
go back to reference Rohr N, Märtin S, Fischer J. Correlations between fracture load of zirconia implant supported single crowns and mechanical properties of restorative material and cement. Dent Mater J. 2017. In press. Rohr N, Märtin S, Fischer J. Correlations between fracture load of zirconia implant supported single crowns and mechanical properties of restorative material and cement. Dent Mater J. 2017. In press.
27.
go back to reference Medeiros IS, Gomes MN, Loguercio AD, Filho LE. Diametral tensile strength and Vickers hardness of a composite after storage in different solutions. J Oral Sci. 2007;49:61–6.CrossRefPubMed Medeiros IS, Gomes MN, Loguercio AD, Filho LE. Diametral tensile strength and Vickers hardness of a composite after storage in different solutions. J Oral Sci. 2007;49:61–6.CrossRefPubMed
28.
29.
go back to reference Ferracane JL. Hygroscopic and hydrolytic effects in dental polymer networks. Dent Mater. 2006;22:211–22.CrossRefPubMed Ferracane JL. Hygroscopic and hydrolytic effects in dental polymer networks. Dent Mater. 2006;22:211–22.CrossRefPubMed
30.
go back to reference Barclay CW, Spence D, Laird WR. Intra-oral temperatures during function. J Oral Rehabil. 2005;32:886–94.CrossRefPubMed Barclay CW, Spence D, Laird WR. Intra-oral temperatures during function. J Oral Rehabil. 2005;32:886–94.CrossRefPubMed
31.
go back to reference Ernst CP, Canbek K, Euler T, Willershausen B. In vivo validation of the historical in vitro thermocycling temperature range for dental materials testing. Clin Oral Investig. 2004;8:130–8.PubMed Ernst CP, Canbek K, Euler T, Willershausen B. In vivo validation of the historical in vitro thermocycling temperature range for dental materials testing. Clin Oral Investig. 2004;8:130–8.PubMed
32.
go back to reference Hahnel S, Henrich A, Bürgers R, Handel G, Rosentritt M. Investigation of mechanical properties of modern dental composites after artificial aging for one year. Oper Dent. 2010;35:412–9.CrossRefPubMed Hahnel S, Henrich A, Bürgers R, Handel G, Rosentritt M. Investigation of mechanical properties of modern dental composites after artificial aging for one year. Oper Dent. 2010;35:412–9.CrossRefPubMed
33.
go back to reference Assunção WG, Gomes EA, Barão VA, Barbosa DB, Delben JA, Tabata LF. Effect of storage in artificial saliva and thermal cycling on Knoop hardness of resin denture teeth. J Prosthodont Res. 2010;54:123–7.CrossRefPubMed Assunção WG, Gomes EA, Barão VA, Barbosa DB, Delben JA, Tabata LF. Effect of storage in artificial saliva and thermal cycling on Knoop hardness of resin denture teeth. J Prosthodont Res. 2010;54:123–7.CrossRefPubMed
34.
go back to reference Weir MD, Moreau JL, Levine ED, Strassler HE, Chow LC, Xu HH. Nanocomposite containing CaF(2) nanoparticles: thermal cycling, wear and long-term water-aging. Dent Mater. 2012;28:642–52.CrossRefPubMedPubMedCentral Weir MD, Moreau JL, Levine ED, Strassler HE, Chow LC, Xu HH. Nanocomposite containing CaF(2) nanoparticles: thermal cycling, wear and long-term water-aging. Dent Mater. 2012;28:642–52.CrossRefPubMedPubMedCentral
35.
go back to reference Kawano F, Ohguri T, Ichikawa T, Matsumoto N. Influence of thermal cycles in water on flexural strength of laboratory-processed composite resin. J Oral Rehabil. 2001;28:703–7.CrossRefPubMed Kawano F, Ohguri T, Ichikawa T, Matsumoto N. Influence of thermal cycles in water on flexural strength of laboratory-processed composite resin. J Oral Rehabil. 2001;28:703–7.CrossRefPubMed
36.
go back to reference Kim AR, Jeon YC, Jeong CM, Yun MJ, Choi JW, Kwon YH, Huh JB. Effect of activation modes on the compressive strength, diametral tensile strength and microhardness of dual-cured self-adhesive resin cements. Dent Mater J. 2016;35:298–308.CrossRefPubMed Kim AR, Jeon YC, Jeong CM, Yun MJ, Choi JW, Kwon YH, Huh JB. Effect of activation modes on the compressive strength, diametral tensile strength and microhardness of dual-cured self-adhesive resin cements. Dent Mater J. 2016;35:298–308.CrossRefPubMed
37.
go back to reference Versluis A, Douglas WH, Sakaguchi RL. Thermal expansion coefficient of dental composites measured with strain gauges. Dent Mater. 1996;12:290–4.CrossRefPubMed Versluis A, Douglas WH, Sakaguchi RL. Thermal expansion coefficient of dental composites measured with strain gauges. Dent Mater. 1996;12:290–4.CrossRefPubMed
38.
go back to reference Morresi AL, D'Amario M, Capogreco M, Gatto R, Marzo G, D'Arcangelo C, Monaco A. Thermal cycling for restorative materials: does a standardized protocol exist in laboratory testing? A literature review. J Mech Behav Biomed Mater. 2014;29:295–308.CrossRefPubMed Morresi AL, D'Amario M, Capogreco M, Gatto R, Marzo G, D'Arcangelo C, Monaco A. Thermal cycling for restorative materials: does a standardized protocol exist in laboratory testing? A literature review. J Mech Behav Biomed Mater. 2014;29:295–308.CrossRefPubMed
39.
go back to reference Nakamura T, Wakabayashi K, Kinuta S, Nishida H, Miyamae M, Yatani H. Mechanical properties of new self-adhesive resin-based cement. J Prosthodont Res. 2010;54:59–64.CrossRefPubMed Nakamura T, Wakabayashi K, Kinuta S, Nishida H, Miyamae M, Yatani H. Mechanical properties of new self-adhesive resin-based cement. J Prosthodont Res. 2010;54:59–64.CrossRefPubMed
Metadata
Title
Effect of aging and curing mode on the compressive and indirect tensile strength of resin composite cements
Authors
Nadja Rohr
Jens Fischer
Publication date
01-12-2017
Publisher
BioMed Central
Published in
Head & Face Medicine / Issue 1/2017
Electronic ISSN: 1746-160X
DOI
https://doi.org/10.1186/s13005-017-0155-z

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